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1 article(s) from Persi, Lorenzo

Synthesis and characterization of water-soluble C₆₀–peptide conjugates

Yue Ma,
Lorenzo Persi and
Yoko Yamakoshi

Beilstein J. Org. Chem. 2024, 20, 777–786, doi:10.3762/bjoc.20.71

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Graphical Abstract

Figure 1: a) Synthesis of C₆₀–oligopeptide conjugates 5a–c and b) synthesis of compound 3. Fulleropyrrolidine...

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Figure 2: Structure of C₆₀–oligo-Lys (5a), C₆₀–oligo-Glu (5b), and C₆₀–oligo-Arg (5c) and images of dissolved...

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Figure 3: DLS diagrams of C₆₀–peptide conjugates 5a (1 mM, in Milli-Q^® water), 5b (1 mM, in Milli-Q^® water or...

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Figure 4: UV–vis spectra of C₆₀–peptide conjugates 5a and 5b (20 μM in Milli-Q^® water for 5a and in pH 9.0 TR...

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Figure 5: ¹H NMR spectrum of C₆₀–peptide conjugate 5a in D₂O (above) and of the precursor monoadduct in CDCl₃...

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Figure 6: ¹³C NMR spectrum of C₆₀–peptide conjugate 5a in D₂O and of the precursor monoadduct in CDCl₃ at 150...

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Figure 7: a) X-band ESR spectra of the 4-oxo-TEMP adduct with ¹O₂ generated by C₆₀–oligo-Lys (5a) and rose be...

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Published 12 Apr 2024

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Synthesis and characterization of water-soluble C60–peptide conjugates

Synthesis and characterization of water-soluble C₆₀–peptide conjugates